Search results for "Equiaxed crystals"
showing 6 items of 6 documents
Nanoscale chemistry and atomic-scale microstructure of a bulk Ni3Sn material built using selective laser melting of elemental powder blends
2021
Abstract Cubic specimens of the intermetallic Ni3Sn compound were built using selective laser melting of elemental powder blends. A specimen built at a laser power of 200 W and a scanning speed of 0.5 m/s was determined to have a homogeneous distribution of Ni and Sn on a mesoscopic scale in spite of a 2 at.% Sn deficiency. Characterization of the microstructure using the HAADF-STEM technique reveals a dispersion of ultrafine Ni particles, nanoscale chemical inhomogeneity and the formation of antiphase nanodomains in the matrix of equiaxed Ni3Sn grains. While a mesoscopic homogeneity of the specimen demonstrates a prospect of additive manufacturing of a bulk intermetallic material using sel…
The Role of Zr in the High-Temperature Oxidation of Fe<sub>3</sub>Al
2008
The paper describes an examination of the effect of the addition of zirconium as a third element on the heat-resisting properties and explains the high temperature oxidation mechanism of Fe3Al intermetallic compounds. The Fe3Al and Fe3Al-0,05Zr specimens have been isothermally oxidized in the temperature range of 1173-1473 K in synthetic air for 100 hrs. The formed oxide layer, about 1,5-2 μm thick, was Al2O3. An examination of the cross-sectioned scales by SEM-EDS showed that the alumina layer consisted of a small inner columnar layer and an outer equiaxed grain layer. Additionally, very fine (50-150 nm) oxide grains rich in Zr, further identified as ZrO2, were found across the alumina sca…
XRD microstructural analysis of mullites obtained from kaolinite–alumina mixtures
2000
Abstract A microstructural study of mullite obtained by the reaction sintering of kaolinite–α–alumina mixtures in the range 1150–1700°C has been performed by using X-ray line profile analyses together with scanning and transmission electron microscopy equipped with microanalysis by energy dispersion (SEM-EDS, TEM-AEM). Two kinds of morphology corresponding to primary (elongated grains) and secondary (equiaxed grains) mullite have been observed. A bimodal crystallite size distribution has been detected through XRD microstructural analysis from 1300°C. The results obtained by this method are compared with SEM/TEM data.
Mechanical properties and microstructural study of homogeneous and heterogeneous laser welds in α, β,and α + β titanium alloys
2018
International audience; Heterogeneous welding has been investigated for three different couples of titanium alloys: α/α + β, α/β,andα + β/β. Plates of 100 × 60 mm and 1.6 or 1.8 mm thick were welded with a Yb:YAG laser. Tensile tests show that the resistance of the heterogeneous welded specimens was generally controlled by those of the weakest material except for the α + β/β where the ultimate tensile strength was approximately equal to the average value of both materials. In every case, the elongation of the welded sample was found to be smaller than that of the base metals. The rupture generally took place outside the weld metal and was found to be most of the time located in the alloy ha…
Towards ductilization of high strength 7XXX aluminium alloys via microstructural modifications obtained by friction stir processing and heat treatmen…
2021
Abstract High strength 7XXX aluminium series reach exceptional strength, higher than all other industrial aluminium alloys. However, they suffer from a lack of ductility compared to softer series. This work presents a procedure to improve the ductility of 7475 Al alloy in high strength condition, reaching a true fracture strain of 70% at full 500 MPa T6 yield strength. Using friction stir processing (FSP) and post-FSP heat treatments, 100% of industrial rolled material T6 yield stress is maintained but a 180% increase in fracture strain is measured for the processed material. This ductility improvement is studied by in-situ synchrotron X-ray tomography and is explained by the reduction of i…
Structure and composition heterogeneity of a FeAl alloy prepared by one-step synthesis and consolidation processing and their influence on grain size…
2006
Abstract This paper aims to characterize a bulk dense FeAl (47 at.%) alloy synthesized and consolidated by one-step current-activated pressure-assisted processing of nanocrystalline elemental powders. The end-product was analyzed using a combination of scanning (SEM) and transmission electron microscopies (TEM), electron back-scattering diffraction (EBSD) as well as electron probe microanalysis (EPMA). Special attention was paid to verify the grain size (32–89 nm) previously determined by X-ray diffraction peak profile analysis. It has been found that this material displays equiaxed grains (0.8–4 μm in size) and contains limited structural defects like subgrains and dislocations. The EPMA r…